›› 2023, Vol. 37 ›› Issue (7): 98-103.

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灰分对PE材料炭黑含量检测的影响

吴海龙1,肖照华2,赵森龙3,李岩4,扈廷勇5   

  1. 1. 梧州学院
    2. 梧州市产品质量检验所
    3. 浙江方圆检测集团股份有限公司
    4. 中国合格评定国家认可中心
    5. 广西五一管业股份有限公司
  • 收稿日期:2023-03-10 修回日期:2023-04-03 出版日期:2023-07-26 发布日期:2023-07-26
  • 基金资助:
    2023年广西自然科学基金项目(面上项目);2020年梧州高新区、梧州学院产学研项目

Effect of ash content on detection of carbon black content in PE materials

  • Received:2023-03-10 Revised:2023-04-03 Online:2023-07-26 Published:2023-07-26

摘要: 采用热失重法,从标准化与生产技术角度分析含灰分聚乙烯(PE)材料炭黑含量检测中存在的问题,指出现行炭黑含量检测方法标准因煅烧条件设置不合理,PE材料灰分在煅烧前后质量存在差异,导致炭黑含量检验结果存在偏差的不足,提出调整煅烧条件,降低煅烧温度的方法,减少煅烧前后灰分的质量变化,消除灰分存在对PE材料炭黑含量检测结果的显著性影响,满足含灰分PE材料炭黑含量检测的现实需要。

关键词: 灰分, 炭黑, 聚乙烯

Abstract: The problems in the detection of carbon black content of ash-containing PE materials were analyzed by thermogravimetry from the view point of standardization and production technology. It should be pointed out that the current detection method of carbon black content was unreasonable due to the unreasonable setting of calcination conditions as well as the difference in the ash content of PE materials existed before and after calcination. Such a difference leads to the shortage of deviation in the test results of carbon black content. A new method was proposed to adjust the calcination conditions and reduce the calcination temperature and the quality change of ash before and after calcination, and eliminate the significant influence of the existence of ash on the test results of carbon black content of PE materials. These can meet the practical requirement for the detection of the carbon black content of ash-containing PE materials.

Key words: ash, carbon black, polyethylene