中国塑料 ›› 2010, Vol. 24 ›› Issue (07): 92-97 .DOI: 10.19491/j.issn.1001-9278.2010.07.020

• 标准与测试 • 上一篇    下一篇

微波爆米花包装袋用微波感受材料中非挥发性紫外可吸收物质迁移行为研究

应璐 王全林 戴双燕 刘志洪   

  1. 宁波市产品质量监督检验所 宁波市产品质量监督检验研究院 宁波市产品质量监督检验研究院
  • 收稿日期:2010-02-26 修回日期:2010-04-13 出版日期:2010-07-26 发布日期:2010-07-26

Study on Migration Behavior of Nonvolatile Ultraviolet Absorbing Extractables from Microwave Susceptors Used in Microwave Popcorn Bags

YING Lu WANG Quanlin DAI Shuangyan LIU Zhihong   

  • Received:2010-02-26 Revised:2010-04-13 Online:2010-07-26 Published:2010-07-26
  • Contact: WANG Quanlin

摘要: 将市售的微波爆米花包装袋用微波感受材料浸入模拟食品玉米油中,在模拟微波条件下加热提取非挥发性紫外可吸收物质。迁移进玉米油中的非挥发性紫外吸收物质经正己烷-乙腈萃取、浓缩、N,N-二甲基乙酰胺定容至2 mL后,以高效液相色谱分离并定量。结果表明,4个样品的迁移量平均值分别为93.3、134.1、38.4和11.8 μg/in2,仅1个样品的迁移量符合美国食品药品监督管理局(FDA)规定的≤20 μg/in2的限量标准。

关键词: 微波爆米花, 微波感受材料, 非挥发性紫外可吸收物, 迁移

Abstract: In this paper, microwave susceptors in the microwave popcorn bags were immerged into corn oil. When the system was heated in a microwave oven, some nonvolatile ultraviolet absorbing species were migrated into the corn oil. Such nonvolatile ultraviolet absorbing species were then extracted by hexane-acetonitrile. With water bath and a gentle nitrogen stream, the extract was dried and concentrated, and subsequently kept as a solution of dimethylacetamide of 2mL. The extract was finally separated with a high performance liquid chromatography and weighed. The weights of the extracts for four samples were 93.3, 134.1, 38.4, and 11.8μg/in2 respectively. Only one of these samples was below the FDA's safety limit standard of 20 μg/in2.

Key words: microwave popcorn, microwave susceptor, nonvolatile ultraviolet absorbing extractables, migration

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