›› 2023, Vol. 37 ›› Issue (5): 15-21.

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固体浮力材料的制备工艺及性能

李涛,黄纬,吴平伟,戴金辉   

  1. 中国海洋大学
  • 收稿日期:2023-02-06 修回日期:2023-02-23 出版日期:2023-05-26 发布日期:2023-05-26
  • 基金资助:
    国家重点研发计划

Preparations and performance of solid buoyancy materials

  • Received:2023-02-06 Revised:2023-02-23 Online:2023-05-26 Published:2023-05-26

摘要: 以深海固体浮力材料的完全国产化为目标,利用中科雅丽科技有限公司生产的牌号为H25HS的空心玻璃微珠(HGMs)为核心原材料,采用自主研发的浇注成型、模压成型、带压固化成型、真空捣打成型和等静压成型方法分别制备了HGMs体积分数为60 %~75 %的环氧树脂(EP)/HGMs复合材料,并对其密度、抗压强度和耐水静压性能进行了综合测试和对比分析。研究结果表明,H25HS体积分数在68 %以下时,适合的成型方法是浇注成型,可以获得安全使用深度大于6 000 m,密度不大于0.58 g/cm3的固体浮力材料;H25HS体积分数为68 %~70 %时,真空捣打成型和等静压成型方法最优,能够获得安全使用深度为2 000~4 000 m,密度0.48~0.52 g/cm3的固体浮力材料。

关键词: 空心玻璃微珠, 浮力材料, 复合材料, 环氧树脂, 成型方法

Abstract: Aiming at the localization of deep?sea solid buoyancy materials, epoxy resin/hollow glass microsphere (HGMs) composites were prepared by using independently developed casting molding, compression molding, curing with pressure, vacuum tamping, and isostatic pressing methods with a domestic produced HGMs (H25HS) as a raw material at volume fractions of 60 %~75 %. The density, compressive strength, and hydrostatic resistance of the as?prepared composites were comparatively investigated. The results indicated that when the volume fraction of H25HS was below 68 %, casting molding was a suitable molding method, with which a solid buoyancy material with a safe?using depth of more than 6 000 m and a density of less than 0.58 g/cm3 was obtained. When the volume fraction of H25HS was 68 %~70 %, vacuum tamping and isostatic pressing were the optimal methods to obtain a solid buoyancy material with a safe?using depth of 2 000~4 000 m and a density of 0.48~0.52 g/cm3.

Key words: hollow glass microsphere, buoyancy material, composite, epoxy resin, forming method